Thermal Denaturations with the Aviv Model 14
[Show All Images]
  1. The Model 14 has two power supplies located on the lower shelf. The power supply to the left controls various subsystems of the instrument. The power supply to the right is one of those subsystems, the UV lamp power supply. To turn on the instrument, begin by turning on the UV lamp power supply only by turning on the "UV lamp" switch. The Xenon lamp has a very large current draw, and all other electrical systems must be off when striking the UV lamp.
    [Show Image] Model 14 power supplies
  2. The "control power on" light will illuminate on the UV lamp power supply. The UV lamp power supply will then begin to draw current in order to charge the capacitor which will be discharged to strike the lamp.
    [Show Image] UV lamp power supply on
  3. When the UV lamp power supply is charged, the "lamp ready" light will illuminate. This is the indication that the UV lamp power supply is ready prepared to strike the lamp.
    [Show Image] UV lamp ready
  4. Strike the UV lamp using the red "ignite lamp" button. There will be an audible crack as the power supply attempts to strike the lamp. If the lamp strikes, the "lamp on" light will illuminate. If the lamp does not strike, you will have to wait until the "lamp ready" light illuminates again before trying to strike the lamp again.
    Warning: If the UV lamp goes off at any time, you must turn off all other systems, in the reverse order they were turned on, before the "lamp ready" light will re-light. You will then have to bring the rest of the instrument and experiment back up from the beginning.
    [Show Image] UV lamp on
  5. With the UV lamp lit, the power to the instrument can be turned on with the center power switch, "CPU/INST." You will not need the visible lamp for monitoring a protein thermal denaturation, there is no need to turn on that lamp.
    [Show Image] CPU/INST on
  6. As the instrument is powering up, press the power button on the desktop computer to begins its boot sequence. Login as Administrator when presented with the login prompt. The password is under the display on a yellow note. Don't worry about the warnings related to invalid/counterfeit copies of Microsoft Windows. The machine is not connected to the network and can't phone home to check license status.
  7. Launch the instrument control program from the "AVIV MODEL 14 SPEC" icon on the left of the desktop. This program will initialize the instrument through a variety self-tests. There will be some motors which run and gears that move, don't be alarmed. It may be two or three minutes, depending on operating system boot status, before the software is ready to respond to your direction.
    [Show Image] AVIV MODEL 14 SPEC
  8. From the "File" menu, select "Read Aviv Macro." In the resulting dialog, select the "tmelt.amc" file. This macro file defines the thermal denaturation experiment. It includes both machine and experiment configuration and allows the same experiment to be run repeatedly.
    [Show Image] Read Aviv Macro...
    [Show Image] tmelt.amc
  9. From the menu, select "Configure Experiment" and change the "Type" of the experiment to "tmelt" in the resulting dialog. This instructs the software to use the settings and follow the directions in the t-melt macro file. Confirm this selection by clicking "Exit/Save Configuration."
    [Show Image] Configure Experiment
    [Show Image] Type: tmelt
    [Show Image] Exit/Save Configuration
  10. Start your experiment by clicking "RUN EXPERIMENT" in the lower left corner of the application. This will launch the "Aviv Macros Command" Window which will guide the instrument through the experiment. From this point, the experiment will run for roughly seven hours, without your assistance or intervention.
    [Show Image] Run Experiment'
    [Show Image] Aviv Macro Commands Window
  11. The "tmelt" macro is programmed to save data to the path "C:\DATA" naming each file by the experiment name, experiment serial number and cell number. You (or your lab assistant) will find your data in "C:\DATA" at the end of your experiment. Do not be alarmed, but when your experiment ends, your data disappear from the data display.
    [Show Image] 'C:\DATA'
Created : 2017-01-26 12:08:28 | Last Updated: 2017-01-26 12:08:28 | Revision: 0 | 41 views